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Preparation and characterization of poly(l-phenylalanine) chiral stationary phases with varying peptide length.
http://hdl.handle.net/10069/20081
http://hdl.handle.net/10069/20081840d4f34-e8e2-4e76-b739-82b2025e0564
名前 / ファイル | ライセンス | アクション |
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JCA1208_242.pdf (225.7 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2008-10-06 | |||||
タイトル | ||||||
タイトル | Preparation and characterization of poly(l-phenylalanine) chiral stationary phases with varying peptide length. | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Chiral stationary phases | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | l-Phenylalanine | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Liquid chromatography | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Peptide length | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Secondary structure | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
Ohyama, Kaname
× Ohyama, Kaname× Oyamada, Kana× Kishikawa, Naoya× Ohba, Yoshihito× Wada, Mitsuhiro× Maki, Toshihide× Nakashima, Kenichiro× Kuroda, Naotaka |
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抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | Three new chiral stationary phases with different lengths of l-phenylalanine peptide were prepared by solid-phase synthesis with tert-butoxycarbonyl (Boc)-l-phenylalanine on silica. The effect of phenylalanine peptide length on enantioselectivity was studied. The best separation of R/S-warfarin was achieved by the chiral stationary phase with intermediate peptide length. These stationary phases were found to exist mainly in alpha-helical conformation by using FT-IR spectra. The end-capping reagents for the N-terminus of the peptide were also evaluated. | |||||
書誌情報 |
Journal of chromatography. A 巻 1208, 号 1-2, p. 242-245, 発行日 2008-10-24 |
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出版者 | ||||||
出版者 | Elsevier | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 00219673 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA10985833 | |||||
PubMed番号 | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | PMID | |||||
関連識別子 | 18817916 | |||||
DOI | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | DOI | |||||
関連識別子 | 10.1016/j.chroma.2008.08.121 | |||||
権利 | ||||||
権利情報 | Copyright (c) 2008 Elsevier Inc. All rights reserved. | |||||
著者版フラグ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
引用 | ||||||
内容記述タイプ | Other | |||||
内容記述 | Journal of Chromatography A, 1208(1-2), pp.242-245; 2008 |