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Conformational studies on peptides having chiral five-membered ring amino acid with two azido or triazole functional groups within the sequence of Aib residues
http://hdl.handle.net/10069/35165
http://hdl.handle.net/10069/35165109583b1-983b-4e05-ae76-a68a13ba069c
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Supple.pdf (83.7 kB)
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Tetra70_8900.pdf (587.2 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2015-03-31 | |||||
タイトル | ||||||
タイトル | Conformational studies on peptides having chiral five-membered ring amino acid with two azido or triazole functional groups within the sequence of Aib residues | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Amino acids | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Chirality | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Conformation analysis | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Helical structures Peptides | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
Oba, Makoto
× Oba, Makoto× Kawabe, Naomi× Takazaki, Hiroomi× Demizu, Yosuke× Doi, Mitsunobu× Kurihara, Masaaki× Suemune, Hiroshi× Tanaka, Masakazu |
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抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | The chiral cyclic α,α-disubstituted α-amino acid, (3R,4R)-1-amino-3,4-diazido-1-cyclopentanecarboxylic acid [(R,R)-Ac5cdN3], was introduced into achiral α-aminoisobutyric acid (Aib) peptides. The azido groups of (R,R)-Ac5cdN3 in the peptides were efficiently converted into 1,2,3-triazole functional groups. FTIR, 1H NMR, and CD spectra revealed that the dominant conformations of all peptides in solution were 310-helical structures without controlling the helical-screw sense. X-ray crystallographic analyses of peptides containing (R,R)-Ac5cdN3 showed that both the right-handed (P) and left-handed (M) 310-helical structures were present in the crystal state. | |||||
書誌情報 |
Tetrahedron 巻 70, 号 46, p. 8900-8907, 発行日 2014-11-18 |
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出版者 | ||||||
出版者 | Elsevier Limited | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 00404020 | |||||
DOI | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | DOI | |||||
関連識別子 | 10.1016/j.tet.2014.09.086 | |||||
権利 | ||||||
権利情報 | c 2014 Elsevier Ltd. | |||||
権利 | ||||||
権利情報 | NOTICE: this is the author’s version of a work that was accepted for publication in Tetrahedron. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Tetrahedron, 70, 46, (2014) | |||||
著者版フラグ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
引用 | ||||||
内容記述タイプ | Other | |||||
内容記述 | Tetrahedron, 70(46), pp.8900-8907; 2014 |