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Chromatographic determination of aliphatic aldehydes in human serum after pre-column derivatization using 2,2′-furil, a novel fluorogenic reagent
http://hdl.handle.net/10069/33615
http://hdl.handle.net/10069/336158d6fa653-75df-4c81-a835-43306440c447
名前 / ファイル | ライセンス | アクション |
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JCA1300_199.pdf (970.5 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2013-09-09 | |||||
タイトル | ||||||
タイトル | Chromatographic determination of aliphatic aldehydes in human serum after pre-column derivatization using 2,2′-furil, a novel fluorogenic reagent | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | 1,2-Di(2-furyl)-1,2-ethanedione (2,2'-furil) | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Aliphatic aldehydes (lipid peroxidation) | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Difurylimidazole derivatives | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Pre-column fluorogenic derivatization | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Serum analysis | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
Fathy, Bakr Ali Marwa
× Fathy, Bakr Ali Marwa× Kishikawa, Naoya× Ohyama, Kaname× Abdel-Mageed, Mohamed Horria× Mohamed, Abdel-Wadood Hanaa× Mohamed, Mohamed Ashraf× Kuroda, Naotaka |
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抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | A novel, highly sensitive and selective fluorimetric liquid chromatographic method for simultaneous determination of medium chain aliphatic aldehydes was developed. The method was based on the derivatization of aliphatic aldehydes with 1,2-di(2-furyl)-1,2-ethanedione (2,2'-furil), a novel fluorogenic reagent, to form highly fluorescent difurylimidazole derivatives. The fluorescence derivatives were separated in less than 20. min on a reversed-phase ODS column using an isocratic elution with a mixture of methanol-water (80:20, v/v%). The detection limits were from 0.19 to 0.50. nM (1-10. fmol/injection) at a signal-to-noise ratio (S/N) of 3. This method was successfully applied for monitoring of aliphatic aldehydes in healthy human sera by a simple pretreatment procedure without interferences from serum constituents. | |||||
書誌情報 |
Journal of Chromatography A 巻 1300, p. 199-203, 発行日 2013-07-26 |
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出版者 | ||||||
出版者 | Elsevier | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 00219673 | |||||
DOI | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | DOI | |||||
関連識別子 | 10.1016/j.chroma.2013.03.033 | |||||
権利 | ||||||
権利情報 | © 2013 Elsevier B.V. | |||||
権利 | ||||||
権利情報 | NOTICE: this is the author’s version of a work that was accepted for publication in Journal of Chromatography A. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Journal of Chromatography A, 1300(2013) | |||||
著者版フラグ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
引用 | ||||||
内容記述タイプ | Other | |||||
内容記述 | Journal of Chromatography A, 1300, pp.199-203; 2013 |