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Separation of Sympathomimetic Amines of Abuse and Related Compounds by Micellar Electrokinetic Chromatography
http://hdl.handle.net/10069/8403
http://hdl.handle.net/10069/8403803db491-4017-4598-9190-691be65ffe00
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
CPBul49_905.pdf (69.9 kB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||
|---|---|---|---|---|---|---|
| 公開日 | 2007-10-12 | |||||
| タイトル | ||||||
| タイトル | Separation of Sympathomimetic Amines of Abuse and Related Compounds by Micellar Electrokinetic Chromatography | |||||
| 言語 | ||||||
| 言語 | eng | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | micellar electrokinetic chromatography | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | sympathomimetic amine | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | phentermine | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | Chinese tea | |||||
| 資源タイプ | ||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
| 資源タイプ | journal article | |||||
| 著者 |
Kuroda, Naotaka
× Kuroda, Naotaka× Sato, Daisuke× Ohyama, Kaname× Wada, Mitsuhiro× Nakahara, Yuji× Nakashima, Kenichiro |
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| 抄録 | ||||||
| 内容記述タイプ | Abstract | |||||
| 内容記述 | Separation of twelve sympathomimetic amines and related compounds by micellar electrokinetic chromatography (MEKC) with UV absorbance detection is described. These amines were well separated within 25 min using 50 mM sodium tetraborate solution containing 15 mM sodium dodecylsulfate (SDS) of pH 9.3 as a running solution and detected at 210 nm. MEKC was performed with an applied voltage of 13 kV at 25 °C using a fused-silica capillary (50 cm×75 mm i.d.) with effective length of 37.5 cm. The detection limits of these compounds were in the range from 4 to 97 fmol/injection at a signal-to-noise ratio (S/N) of 3. The reproducibility of the method expressed as relative standard deviation (RSD) for within-day (n=6) and between-day (n=5) assays was less than 4.8 and 8.8%, respectively. The proposed method could be applied to the determination of an anorectic drug, phentermine, in Chinese tea with a detection limit of 99 μg/g (105 fmol/injection, S/N=3). | |||||
| 書誌情報 |
Chemical & Pharmaceutical Bulletin 巻 49, 号 7, p. 905-908, 発行日 2001-07 |
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| 出版者 | ||||||
| 出版者 | Pharmaceutical Society of Japan | |||||
| ISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 00092363 | |||||
| EISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 1347-5223 | |||||
| 書誌レコードID | ||||||
| 収録物識別子タイプ | NCID | |||||
| 収録物識別子 | AA00602100 | |||||
| PubMed番号 | ||||||
| 関連タイプ | isIdenticalTo | |||||
| 識別子タイプ | PMID | |||||
| 関連識別子 | 11456100 | |||||
| DOI | ||||||
| 関連タイプ | isIdenticalTo | |||||
| 識別子タイプ | DOI | |||||
| 関連識別子 | 10.1248/cpb.49.905 | |||||
| 著者版フラグ | ||||||
| 出版タイプ | VoR | |||||
| 出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
| 関係URI | ||||||
| 関連名称 | http://dx.doi.org/10.1248/cpb.49.905 | |||||
| 引用 | ||||||
| 内容記述タイプ | Other | |||||
| 内容記述 | Chemical & Pharmaceutical Bulletin v.49(7) p.905-908, 2001 | |||||
