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Characterization and Comparison of Methacrylic Acid with 2-Acrylamido-2-methyl-1-propanesulfonic Acid in the Preparation of Monolithic Column for Capillary Electrochromatography
http://hdl.handle.net/10069/32396
http://hdl.handle.net/10069/32396c1637a2e-9e6f-4d2f-b8a0-7eaa9364d86d
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
JCS51_425.pdf (910.4 kB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||
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| 公開日 | 2014-06-01 | |||||
| タイトル | ||||||
| タイトル | Characterization and Comparison of Methacrylic Acid with 2-Acrylamido-2-methyl-1-propanesulfonic Acid in the Preparation of Monolithic Column for Capillary Electrochromatography | |||||
| 言語 | ||||||
| 言語 | eng | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | Capillary electrochromatography | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | Butyl methacrylate-based monolith | |||||
| キーワード | ||||||
| 主題Scheme | Other | |||||
| 主題 | Methacrylic acid | |||||
| 資源タイプ | ||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
| 資源タイプ | journal article | |||||
| 著者 |
Horiguchi, Daisuke
× Horiguchi, Daisuke× Ohyama, Kaname× Masunaga, Tomoko× Fujita, Yoshiko× Ali, Marwa Fathy Bakr× Kishikawa, Naoya× Kuroda, Naotaka |
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| 抄録 | ||||||
| 内容記述タイプ | Abstract | |||||
| 内容記述 | Butyl methacrylate (BMA)-ethylene dimethacrylate (EDMA)-methacrylic acid (MAA) and BMA-EDMA-2-acrylamido-2-methyl-1-propanesulfonic acid (AMPS) monolithic columns were prepared by varying the percentage of ionic monomers for capillary electrochromatography. Monolithic columns with a higher content of ionic monomers provided better column efficiency, and the performance of BMA-EDMA-MAA monoliths was better than BMA-EDMA-AMPS. To characterize and optimize BMA-EDMA-MAA monoliths, the effects of the content of cross-linker and the total monomer in the polymerization mixture on column performance were also studied. Plate heights of 8.2μm for the unretained solute (thiourea) and 12.6μm for the retained solute (naphthalene) were achieved with a monolithic column using 2.5% MAA (Column I). | |||||
| 書誌情報 |
Journal of Chromatographic Science 巻 51, 号 5, p. 425-429, 発行日 2013-05 |
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| 出版者 | ||||||
| 出版者 | Oxford University Press | |||||
| ISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 00219665 | |||||
| EISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 1945239X | |||||
| DOI | ||||||
| 関連タイプ | isVersionOf | |||||
| 識別子タイプ | DOI | |||||
| 関連識別子 | 10.1093/chromsci/bms158 | |||||
| 権利 | ||||||
| 権利情報 | © 2012 Published by Oxford University Press. All rights reserved. | |||||
| 権利 | ||||||
| 権利情報 | This is a pre-copy-editing, author-produced PDF of an article accepted for publication in Journal of Chromatographic Science following peer review. The definitive publisher-authenticated version Journal of Chromatographic Science, 51 (5), pp. 425-429; 2013 is available online at: http://dx.doi.org/10.1093/chromsci/bms158 | |||||
| 著者版フラグ | ||||||
| 出版タイプ | AM | |||||
| 出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
| 引用 | ||||||
| 内容記述タイプ | Other | |||||
| 内容記述 | Journal of Chromatographic Science, 51(5), pp.425-429; 2013 | |||||
